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Bonert and Pohl reported results for the atomic absorption analysis of several metals in the caustic suspensions produced during the manufacture of soda by the ammonia-soda process. ^31 (a) The concentration of Cu is determined by acidifying a 200.0-mL sample of the caustic solution with 20  mL of concentrated HNO3, adding 1  mL of 27 % w / v H2 O2, and boiling for 30  min . The resulting solution is diluted to 500  mL in a volumetric flask, filtered, and analyzed by flame atomic absorption usin
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